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By D.R. UHLMANN and N.J. KREIDL (Eds.)

ISBN-10: 0127067043

ISBN-13: 9780127067049

ISBN-10: 0127067078

ISBN-13: 9780127067070

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While a-GeS 2 appears to have a 4:2 coordination arrangement like a-GeSe2, germanium is reported to be threefold coordinated in a-GeS—realizing a prediction made by Bienenstock on the basis of conventional X-ray diffraction measurements (1973). Fuoss and colleagues came to the same conclusions for a-GeSe in their anomalous dispersion studies. Interestingly, c-GeS and c-GeSe have distorted rock-salt structures, characterized by extensive mesomeric bonding arrangements. The similarity between these structures and that of black phosphorous has been made (Bienenstock, 1983).

In a-As 2 S 3 Se 3 Pettifer found arsenic had both selenium and sulphur nearest neighbors. These were in the ratio 1:2, but at the expected covalent distances found in the binary glasses (Pettifer, 1979). The heteropolar bonding reported in arsenic sulphides and selenides contrasts with the situation found in a-As 2 Te 3 , where evidence for homopolar bonding has been found (Gurman, 1988). 53A. While the local environment displays some chemical disorder, the network is essentially threefold coordinated in marked contrast to crystalline As 2 Te 3 where arsenic occupies three- and sixfold sites.

N. GREAVES ordering and random bonding in what is already a structurally disordered solid. /. Glass Former Environments in a-Ge02, a-Si02, and Binary Glasses The EXAFS Fourier transforms of the K-edge of Ge are shown in Fig. 8 for vitreous Ge0 2 (3) and two of its crystalline polymorphs: a-quartz form (2) and rutile form (1). These are the results of Lapeyre and coworkers (1983) and demonstrate how the first and second shells of atoms in the glass closely match in position the tetrahedral Ge sites in the a-quartz structure.

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Advances in Structural Analysis by D.R. UHLMANN and N.J. KREIDL (Eds.)

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